Stabilization heat treatment and functional response of 0.65[Pb(Mg1/3Nb2/3)O3]-0.35[PbTiO3] ceramics

Pius Augustine; Shibnath Samanta; Martando Rath; Muralidhar Miryala; K. Sethupathi; Masato Murakami; M. S. Ramachandra Rao

doi:10.1016/j.materresbull.2017.07.019

Stabilization heat treatment and functional response of 0.65[Pb(Mg_1/3Nb_2/3)O₃]-0.35[PbTiO₃] ceramics

Pius Augustine, Shibnath Samanta, Martando Rath, Muralidhar Miryala, K. Sethupathi, Masato Murakami, M. S. Ramachandra Rao

Research output: Contribution to journal › Article › peer-review

7 Citations (Scopus)

Abstract

We report on the heat treatment to stabilize 0.65[Pb(Mg_1/3Nb_2/3)O₃]-0.35[PbTiO₃] ceramics and its effect on the functional response. The stabilization heat treatment at 1050 °C for 4 h was effective in removing un-reacted PbO from the ceramics, which was confirmed through the measurements of dielectric and ferroelectric properties for a series of samples with different PbO contents. We also found that the stage of the stabilization heat treatment affected the sample properties. When this treatment was administrated to the sample during calcination, it exhibited excellent ferroelectric behavior. On the other hand, the same stabilization heat treatment given to the compacted pellet prior to sintering resulted in excellent dielectric properties with comparatively low ferroelectric hysteresis.

Original language	English
Pages (from-to)	47-55
Number of pages	9
Journal	Materials Research Bulletin
Volume	95
DOIs	https://doi.org/10.1016/j.materresbull.2017.07.019
Publication status	Published - 2017 Nov

Keywords

A. Ceramics
B. Microstructure
B. Piezoelectricity
D. Dielectric properties
D. Ferroelectricity

ASJC Scopus subject areas

Materials Science(all)
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Access to Document

10.1016/j.materresbull.2017.07.019

Cite this

@article{42724e89823b46d5ada49117d50157b3,

title = "Stabilization heat treatment and functional response of 0.65[Pb(Mg1/3Nb2/3)O3]-0.35[PbTiO3] ceramics",

abstract = "We report on the heat treatment to stabilize 0.65[Pb(Mg1/3Nb2/3)O3]-0.35[PbTiO3] ceramics and its effect on the functional response. The stabilization heat treatment at 1050 °C for 4 h was effective in removing un-reacted PbO from the ceramics, which was confirmed through the measurements of dielectric and ferroelectric properties for a series of samples with different PbO contents. We also found that the stage of the stabilization heat treatment affected the sample properties. When this treatment was administrated to the sample during calcination, it exhibited excellent ferroelectric behavior. On the other hand, the same stabilization heat treatment given to the compacted pellet prior to sintering resulted in excellent dielectric properties with comparatively low ferroelectric hysteresis.",

keywords = "A. Ceramics, B. Microstructure, B. Piezoelectricity, D. Dielectric properties, D. Ferroelectricity",

author = "Pius Augustine and Shibnath Samanta and Martando Rath and Muralidhar Miryala and K. Sethupathi and Masato Murakami and {Ramachandra Rao}, {M. S.}",

note = "Publisher Copyright: {\textcopyright} 2017 Elsevier Ltd",

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T1 - Stabilization heat treatment and functional response of 0.65[Pb(Mg1/3Nb2/3)O3]-0.35[PbTiO3] ceramics

AU - Augustine, Pius

AU - Samanta, Shibnath

AU - Rath, Martando

AU - Miryala, Muralidhar

AU - Sethupathi, K.

AU - Murakami, Masato

AU - Ramachandra Rao, M. S.

PY - 2017/11

Y1 - 2017/11

N2 - We report on the heat treatment to stabilize 0.65[Pb(Mg1/3Nb2/3)O3]-0.35[PbTiO3] ceramics and its effect on the functional response. The stabilization heat treatment at 1050 °C for 4 h was effective in removing un-reacted PbO from the ceramics, which was confirmed through the measurements of dielectric and ferroelectric properties for a series of samples with different PbO contents. We also found that the stage of the stabilization heat treatment affected the sample properties. When this treatment was administrated to the sample during calcination, it exhibited excellent ferroelectric behavior. On the other hand, the same stabilization heat treatment given to the compacted pellet prior to sintering resulted in excellent dielectric properties with comparatively low ferroelectric hysteresis.

AB - We report on the heat treatment to stabilize 0.65[Pb(Mg1/3Nb2/3)O3]-0.35[PbTiO3] ceramics and its effect on the functional response. The stabilization heat treatment at 1050 °C for 4 h was effective in removing un-reacted PbO from the ceramics, which was confirmed through the measurements of dielectric and ferroelectric properties for a series of samples with different PbO contents. We also found that the stage of the stabilization heat treatment affected the sample properties. When this treatment was administrated to the sample during calcination, it exhibited excellent ferroelectric behavior. On the other hand, the same stabilization heat treatment given to the compacted pellet prior to sintering resulted in excellent dielectric properties with comparatively low ferroelectric hysteresis.

KW - A. Ceramics

KW - B. Microstructure

KW - B. Piezoelectricity

KW - D. Dielectric properties

KW - D. Ferroelectricity

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