TY - JOUR
T1 - Subgrain structures in RE123 bulk superconductors
AU - Ogasawara, Kei
AU - Sakai, Naomichi
AU - Murakami, Masato
PY - 2002/4
Y1 - 2002/4
N2 - We have studied the microstructures of subgrains in large-grain RE123 (RE = Y, Sm) bulk superconductors through microscopic observation and x-ray pole figure analyses. For the samples grown by slow-cooling, misorientation of the subgrains increases along with the crystal growth, and also that the misorientation has positive relation to the size and concentration of the second-phase particles. For isothermally grown samples, subgrains are likely to form under large undercooling. We discuss the possible mechanism of subgrain formation. Such subgrains are considered to affect current carrying capabilities in bulk materials, so that we performed magnetic and electric measurements for several samples having different subgrain structures. The results of Jc-B and AC transport measurements indicated that the subgrains act as weak-links, especially under high magnetic fields.
AB - We have studied the microstructures of subgrains in large-grain RE123 (RE = Y, Sm) bulk superconductors through microscopic observation and x-ray pole figure analyses. For the samples grown by slow-cooling, misorientation of the subgrains increases along with the crystal growth, and also that the misorientation has positive relation to the size and concentration of the second-phase particles. For isothermally grown samples, subgrains are likely to form under large undercooling. We discuss the possible mechanism of subgrain formation. Such subgrains are considered to affect current carrying capabilities in bulk materials, so that we performed magnetic and electric measurements for several samples having different subgrain structures. The results of Jc-B and AC transport measurements indicated that the subgrains act as weak-links, especially under high magnetic fields.
KW - Bulk superconductor
KW - Micro-area x-ray diffraction
KW - Polarized optical microscopy
KW - Pole figure
KW - RE123
KW - Subgrain
KW - Superconducting properties
KW - Transmission electron microscopy
KW - Weak-link
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U2 - 10.2320/jinstmet1952.66.4_302
DO - 10.2320/jinstmet1952.66.4_302
M3 - Article
AN - SCOPUS:0036543434
SN - 0021-4876
VL - 66
SP - 302
EP - 308
JO - Nippon Kinzoku Gakkaishi/Journal of the Japan Institute of Metals
JF - Nippon Kinzoku Gakkaishi/Journal of the Japan Institute of Metals
IS - 4
ER -